Penulis Utama : Angga Eryanto Putro
Penulis Tambahan : -
NIM / NIP : M0309005
Tahun : 2015
Judul : Studi Reaksi Ploroglusinol dengan Etil 2-Kloro Asetat
Edisi :
Imprint : Surakarta - FMIPA - 2015
Kolasi :
Sumber : UNS-FMIPA Jur. Pendidikan Kimia-M0309005-2015
Subyek : REAKSI PLOROGLUSINOL
Jenis Dokumen : Skripsi
ISSN :
ISBN :
Abstrak :

ABSTRAK
Reaksiploroglusinoldenganetil 2-kloro asetattelahselesaidipelajari. Tujuanpenelitianiniadalahmembentuksenyawaturunanploroglusinoldenganmereaksikanploroglusinoldenganetil 2-kloro asetatsecaraberlebih.
Reaksiploroglusinolmenggunakanetil 2-kloro asetatdilakukandenganrefluksselama 24 jam padasuhu 56oC. Produkreaksidiidentifikasidenganmenggunakankromatografi lapis tapisdandilakukankarakterisasidenganujititikleleh. Analisisstrukturprodukyang diperolehdenganspektrofotometer FTIR, 1H-NMR, dan13C-NMR.
Hasilreaksiantaraploroglusinoldanetil 2-kloro asetatmerupakanpadatanhitamkecoklatandanmempunyaititiklelehsebesar 191oC. Berdasarkananalisisstrukturdengan FTIR, 1H-NMR dan13C-NMR, produkreaksiberupacampuransenyawayaituetil 2-(3,5-dihidroksifenol) asetat,  etil 2-(2,4,6-trioksosikloheksil) asetat, dansisaploroglusinol yang belumbisabereaksi.
Kata kunci:Etil 2-kloro asetat, Ploroglusinol.
ABSTRACT
Reaction between phloroglucinoland 2-chloro ethyl acetate has been studied. The purpose of this study was to establish phloroglucinol derivatives by reacting phloroglucinol with ethyl 2-chloro acetate in excess.
Phloroglucinol reaction using 2-chloro ethyl acetate was carried out under reflux for 24 hours at a temperature of 56oC. The reaction products were identified by a thin layer chromatography and were characterized by melting point test. Analysis of the structure of the products was obtained by FTIR spectrophotometer, 1H-NMR and 13C-NMR.
The result of the reaction between phloroglucinol and 2-chloro ethyl acetate was brownish black solid and has a melting point of 191oC. Based on the structural analysis by FTIR, 1H-NMR and 13C-NMR, the reaction product was a mixture of compounds which is ethyl 2- (3,5-dihidroksifenol) acetate, ethyl 2-(2,4,6-trioxosikloheksil) acetate, and the rest of phloroglucinol which can not react.
Keywords: 2-chloro ethyl acetate, Phloroglucinol.

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Status : Public
Pembimbing : 1. Dr. Triana Kusumaningsih, M. Si.
2. Dr. Desi Suci Handayani, M.Si.
Catatan Umum :
Fakultas : Fak. MIPA